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Cake day: August 8th, 2023

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  • skillissuer@discuss.tchncs.detoScience Memes@mander.xyz2 Kinds
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    25 days ago

    one small integer is not enough, two small integers are better (lab journal initials/number and sample number, like AC7-295. something like AC7-295A, then AC7-295B and so on if needed. that’s how i do it anyway) this way there’s no possibility of mixup with other people’s samples and samples described in old lab journals






  • Almost all of solvents are made from petrochemicals, so it’s a distinction without difference. Few exceptions (bioethanol, MeTHF, DMSO maybe) also require obscene amounts of energy to prepare

    What makes acetone tick as a solvent is the fact that most of phenol is used up immediately for bisphenol A, and this leaves 1eq of acetone from cumene process unused (or cyclohexanone, and this leaves all acetone unused). In some way, acetone is a waste product and that’s why PMMA or isophorone diamine is a thing

    Just it’s low toxicity, the fact it’s non-chlorinated and sane boiling point makes acetone a pretty green solvent by comparison









  • Like, so what if we store our tBuLi with other low-flash point flammables? And pyrophoric oxidizers? In the same bin? That’s stuck in a block of ice because in the 30-year-old freezer because it hasn’t ever been de-iced?

    That’s just bad management and you shouldn’t store tBuLi that long anyway because it’ll decompose. You shouldn’t put it in freezer either

    Oh, while you’re here, does this still smell like DCM? I can’t tell if I rotavapped it all off and the NMR tubes all need aqua regia (sorry my b).

    just put it on high vacuum

    What are you working with that requires aqua regia to clean NMR tubes? I’ve only had to use piranha once in a decade, while cleaning things that acetone, DCM, and basic ethanol won’t touch, and this was just after moving to another lab